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Beilstein J. Org. Chem. 2013, 9, 2009–2014, doi:10.3762/bjoc.9.236
Graphical Abstract
Scheme 1: Synthesis of optically active N-acyloxazolidinone 5 from 4,4,4-trifluorobutanoic acid. Conditions: ...
Scheme 2: Synthesis of enantiomerically pure (2S,3S)-5-F3Ile and (2R,3S)-5-F3-allo-Ile. TMGA = 1,1,3,3-tetram...
Figure 1: Retention times of Fmoc amino acids plotted against the van der Waals volume of their side chains. ...
Figure 2: CD spectra of K-5-F3Ile and K-Ile peptides (KX: Ac-YGGKAAAAKAXAAKAAAAK-NH2). The K-4’-F3Ile spectru...